摘要
采用硝酸-双氧水对槲寄生全药及煎煮液进行湿法消解,用电感耦合等离子体原子发射光谱法(ICP-AES)同时测定试样中Cu,Mg,Zn,Mn,Ni,Se,K,Na,Ca和Fe等元素的含量。该法的的加标回收率为91.6%~108.9%,变异系数为0.47%~4.59%,具有良好的准确度和精密度。结果表明:槲寄生中含有丰富的K和Ca元素,Na和Mg的含量也相对丰富,为进一步研究槲寄生的药理提供了科学的数据。
A method for the simultaneous determination of elements Cu, Mg, Zn, Mn, Ni, Se, K, Na, Ca and Fe in mistletoe after HNCh-H2O2 digestion by ICt-AES was studied. The recoveries obtained by standard addition method were between 90. 8% and 112. 8%, while the RSD (n=5) was in the range of 0.47%-4. 59%. The results showed that there were rich K, Ca, Mg and Na in the mistletoe, and offered scientific data for the ulterior study on mistletoe.
出处
《光谱学与光谱分析》
SCIE
EI
CAS
CSCD
北大核心
2008年第5期1157-1159,共3页
Spectroscopy and Spectral Analysis
基金
国家自然科学基金项目(20365002)
长江学者和创新团队发展计划项目(IRT0540)资助