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GC/MS法测定环境空气中痕量POPs类有机氯农药及降解产物 被引量:8

Determination of Trace Organo-Chlorine Pesticides and Their Degradative Products in Ambient Air by GC/MS
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摘要 采用快速溶剂萃取-氟罗里硅土柱净化-气相色谱/质谱联用法测定环境空气中POPs类有机氯农药及其降解产物。艾氏剂、狄氏剂、异狄氏剂、六六六、滴滴涕、七氯、氯丹、灭蚁灵及其降解产物的检出限为2.0 ng~4.6 ng,空白加标回收率为62.1%~118%,RSD为6.8%~15.2%。 A method was established to determine organo-chlorine pesticides of POPs and their degradative products in the ambient air by accelerated solvent extraction-florisil purify-GC/MS. The detection limits of drinox, dieldrin, endrin, BHC, DDT, heptamul, chlordane, dechlorane and their degradative products were from 2.0 ng to 4.6 ng. The blank recoveries were from 62.1% to 118% and the RSD were from 6.8% to 15.2%.
作者 李娟 章勇
出处 《环境监测管理与技术》 北大核心 2008年第6期33-36,共4页 The Administration and Technique of Environmental Monitoring
关键词 有机氯农药 降解产物 GC/MS法 环境空气 Organo-chlorine pesticides Degradation product GC/MS Ambient air
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