期刊文献+

响应面制备辛烯基琥珀酸淀粉酯的工艺研究 被引量:1

Synthesis of starch octenyl succinate anhydride by response surface analysis
下载PDF
导出
摘要 通过响应面分析(Response surface analysis,RSA)软件,采用boxbehnken中心组合设计方法对辛烯基琥珀酸淀粉酯(SSOS)的制备工艺条件进行优化,得到制备辛烯基琥珀酸淀粉酯的最佳工艺条件为:反应温度为34℃,时间1.5h,pH值为8.7,辛烯基琥珀酸酐添加量为淀粉干基的3%,反应取代度(DS)可达0.0144。 Octenyl succinic anhydride (OSA) modified waxy com starch was prepared in aqueous slurry systems with the Box-Behnken in the RSA software. According to the central composite test design principles, the method of response surface method (RSM) with 4 factors and 3 levels was adopted. Response surface and contour are finally graphed with the degree of substitution (DS) as the response value. The suitable parameters were as follows: reaction temperature 34℃, reaction period 1.5h, pH of reaction system 8.7, amount of OSA 3% (in proportion to dry starch). The degree of substitution was 0.0144.
出处 《中国酿造》 CAS 北大核心 2009年第11期95-97,共3页 China Brewing
关键词 辛烯基琥珀酸淀粉酯 响应面 取代度 OSA modified waxy corn starch response surface method the degree of substitution
  • 引文网络
  • 相关文献

参考文献6

二级参考文献46

  • 1OB沃慈堡[美].变性淀粉的性能与应用[M].,.167-169.
  • 2陈熙 张燕萍.无锡轻工大学学报:食品与生物技术,2000,19(5):495-497.
  • 3Barndt Richard L, Zwiercan Gary A, Trubiano Paolo C. United States Patent, 4460617. 1984.
  • 4Mahmoud I, Mahmoud E. United State Patent,4670268. 1987.
  • 5Marotta N G, Boettger R M, Nappen B H. United States Patent, 3455838. 1969.
  • 6Otto B Wurzburg. United States Patent,3499962.1970.
  • 7Anandaraman S. Package Process, 1980, 2 (5) :14.
  • 8Balassa L L, Fanger G O. CRC Crit. Rev. Food Technol., 1971, 7(3) :245--261.
  • 9Graves R E. Cereal Sci. Today, 1972, 17(4):107.
  • 10Caldwell C G, Hills F, Otto B W. United State Patent, 2661349. 1953.

共引文献122

同被引文献14

  • 1薛友林,木泰华,孙艳丽.甘薯蛋白研究进展[J].食品研究与开发,2005,26(5):180-184. 被引量:21
  • 2陆杨,邬应龙,曾珍.响应面法优化琥珀酸淀粉酯制备条件的研究[J].食品与发酵工业,2007,33(5):54-59. 被引量:5
  • 3CALDWELL CG, HILLS F, OTTO BW. Polysaccharide derivatives of substituted dicarboxylic acids[P]. United State Patent, 2661349, 1953.
  • 4JEON YS, LOWER AV, GROSS RA, et al. Studies of starch esterification, reactions with alkenyl sueeinates in aqueous slurry systems [J]. Starch, 1999, 51 (1-2) : 90-93.
  • 5PARKA S, CHUNGB MG, YOOA B. Effect of octenylsuccinylation on rheological properties of corn starch pastes [J]. Starch, 2004, 56 (9) : 399-406.
  • 6CHUNG MD, LIM BM. Physiochemical properties of octenylsuccinated corn starch[J]. J Fd Hyg Safety, 1999, 14: 84-89.
  • 7BOX EP, HUNTER WG. Statistics for experiments: An introduction to design, data analysis and model building[M]. New York: Wiley, 1990.
  • 8HUI R, QI-HE C, MING-LIANG F, et al. Preparation and properties of octenyl succinic anhydride modified potato starch [J]. Food Chem, 2009, 114(1) : 1-86.
  • 9王红亮 冯光炷.长链脂肪酸淀粉酯合成及心用研究进展.化学进展,2005,25(7):760-761.
  • 10费荣昌.试验设计与数据处理[M].无锡:江南大学出版社,2001.59-63.

引证文献1

二级引证文献1

;
使用帮助 返回顶部