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在线凝胶色谱串联气相色谱-质谱对食品中七种杀菌剂残留量的测定 被引量:13

Determination of 7 Bactericidals Residues in Food by On-line GPC-GC-MS Method
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摘要 The determination of 7 bactericidals residues,including chlorthalonil,dichlofluanid,tolylfluanid,captan,folpet,captafol and deltamethrin,in foods by using on-line gel permeation chromatography(GPC) coupled with gas chromatography-mass spectrometry(GC-MS).Bactericidal residues were extracted with acetonitrile,and cleaned up by ENVI-Crab,LC-NH2 column and GPC,respectively.The analysis of 7 bactericidals residues was performed by GC-MS.The average recoveries of analytes were range of 75%-120% with RSD of 3.5%-10.3%. The determination of 7 bactericidals residues,including chlorthalonil,dichlofluanid,tolylfluanid,captan,folpet,captafol and deltamethrin,in foods by using on-line gel permeation chromatography(GPC) coupled with gas chromatography-mass spectrometry(GC-MS).Bactericidal residues were extracted with acetonitrile,and cleaned up by ENVI-Crab,LC-NH2 column and GPC,respectively.The analysis of 7 bactericidals residues was performed by GC-MS.The average recoveries of analytes were range of 75%-120% with RSD of 3.5%-10.3%.
出处 《分析测试学报》 CAS CSCD 北大核心 2008年第S1期140-142,共3页 Journal of Instrumental Analysis
关键词 GC-MS BACTERICIDAL RESIDUES GC-MS bactericidal residues
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