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热重法研究脱羧反应中MgO/浮石催化剂的积炭行为 被引量:1

COKE DEPOSITS OF MgO/PUMICE CATALYST IN DECARBOXYLATION BY THERMOGRAVIMETRY
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摘要 利用热重技术考察了反应温度和MgO含量对癸酸与醋酸合成甲基壬基酮MgO/浮石催化剂积炭的影响。确证镁盐流失不是积炭的直接原因,而反应温度对积炭有明显影响,适当调整反应温度可减少积炭的生成。 The influences of reaction temperature and amount of MgO inMgO/pumice catalyst on the coke deposits during the conversion of mixture ofdecanoic acid with acetic acid to methyl n-nonyl ketone have been examined bythemogravimetry. It is obvious that the reaction temperature, not the loss ofMgO in MgO/pumice has an influence on the coke deposits which can be decre-ased with proper reaction temperature,
出处 《中国医药工业杂志》 CAS CSCD 北大核心 1990年第8期370-373,共4页 Chinese Journal of Pharmaceuticals
关键词 甲基壬基酮 合成 热重法 积炭 thermogravimetry MgO/pumice catalyst coke deposits
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