摘要
用气相色谱TCD和FID检测器对多氯乙酰氯及其酯化产物的成分和纯度进行了分析。用正丙醇对其进行衍生化 ,酯化率大于 99.6 % ,生成的酯化产物用毛细管色谱法分析 ,其方法的分离效率高 ,重现性好 ,检测结果准确可靠 ,9次分析的变异系数 0 .45 % ,在工业产品的检测中取得满意的结果。
Component and content of multichloracetyl chloride was analysized by two gas chromatographic methods.The efficiency of separation of capillary gas chromatography analysizing esterification derivatives is high.DSP is good,result of determination is accurate and reliable,multichloracetyl chloride was analysized using thermal conduct detector directly too.
出处
《山东化工》
CAS
2002年第1期43-44,共2页
Shandong Chemical Industry
