摘要
目的建立通林片的中柚皮苷的含量测定方法。方法在Lichrospher5-C184．6mm×25cm柱上，甲醇-0．4％磷酸溶液（40：60）为流动相，检测波长为波长为283nm，流速为1．0ml·min。结果柚皮苷的量在0．3—1．5μg范围内呈良好的线性关系（r=0．9995），回归方程为A=2295380C-66402。精密度试验RSD为0．71％，该方法平均回收率为98．43％，RSD=1．63％。结论该方法简单、快速、准确。
Aim To determine naringin in tongling tablet by HPLC. Methods Lichrospher5-C18 column was used, methanol-0. 4 % phosphate solvent as mobile phase, UV detector at wavelength 283 nm. Results The naringin curvers were linear between 0.3 - 1.5 μg（ r = 0. 9995）. The mean recovery was 98.43 % ,and the RSD was 1.6%. Conclusion This method is simple, quick, and accurate.
出处
《安徽医药》
CAS
2006年第8期585-586,共2页
Anhui Medical and Pharmaceutical Journal
