期刊文献+

Synthesis and Crystal Structure of 4-Bromo-5-ethoxy-3-methyl-5- (naphthalen-1-yl)-1-tosyl-1H-pyrrol-2(5H)-one

Synthesis and Crystal Structure of 4-Bromo-5-ethoxy-3-methyl-5- (naphthalen-1-yl)-1-tosyl-1H-pyrrol-2(5H)-one
下载PDF
导出
摘要 The title compound 4-bromo-5-ethoxy-3-methyl-5-(naphthalen-l-yl)-l-tosyl-lH- pyrrol-2(5H)-one 1 (C24H22BrNO4S, Mr = 500.40) has been synthesized and its crystal structure was determined by single-crystal X-ray diffraction analysis. It crystallizes in monoclinic, space group P21/n with a = 8.8562(15), b = 18.118(3), c = 14.055(2)A, β = 99.855(3)^o, V= 2221.9(6)A3, Z = 4, Dc = 1.496 g/cm^3,μ= 1.975 mm^-1, 2 = 0.71073A, F(000) = 1024, R = 0.0607 and wR = 0.1371. The title compound 4-bromo-5-ethoxy-3-methyl-5-(naphthalen-l-yl)-l-tosyl-lH- pyrrol-2(5H)-one 1 (C24H22BrNO4S, Mr = 500.40) has been synthesized and its crystal structure was determined by single-crystal X-ray diffraction analysis. It crystallizes in monoclinic, space group P21/n with a = 8.8562(15), b = 18.118(3), c = 14.055(2)A, β = 99.855(3)^o, V= 2221.9(6)A3, Z = 4, Dc = 1.496 g/cm^3,μ= 1.975 mm^-1, 2 = 0.71073A, F(000) = 1024, R = 0.0607 and wR = 0.1371.
出处 《Chinese Journal of Structural Chemistry》 SCIE CAS CSCD 北大核心 2007年第12期1505-1508,共4页 结构化学(英文)
基金 This work was supported by the National Natural Science Foundation of China (No. 20472072 and 20332060) the CAS Academician Foundation of Zhejiang Province
关键词 4-bromo-5-ethoxy-3-methyl-5-(naphthalen-1-y1)-1-tosyl-1H-pyrrol-2(5H)-one synthesis crystal structure 4-bromo-5-ethoxy-3-methyl-5-(naphthalen-1-y1)-1-tosyl-1H-pyrrol-2(5H)-one,synthesis, crystal structure
  • 相关文献

参考文献11

  • 1Konig, G M.; Wright, A. D. Planta Med. 1996, 62, 193-211.
  • 2Pietra, E Nat. Prod. Rep. 1997, 14, 453-464.
  • 3Osterhage, C.; Kamlnsky, R.; Koenlg, G M:; Wright, A. D. J. Org. Chem. 2000, 65, 6412 -6417.
  • 4Yamaguchi, J.; Kakeya, H.; Uno, T.; Shoji, M.; Osada, H.; Hayashi, Y. Angew. Chem, Int. Ed, Engl. 2005, 40, 3110-3115.
  • 5Kosugi, Y., Hamaguchi, E Heterocycles 1984, 22, 2363-2368.
  • 6Kinoshlta, H.; Hammam M. A. S.; Inomata, K. Chem. Lett. 2005, 34, 800-801.
  • 7Nikitin, K. V.; Andryukhova, N. E Can. J. Org. Chem. 2004, 82, 571-578.
  • 8Hardcastle, I. R.; Ahmed, S. U.; Atkins, H.; Farnie, G; Goldlng, B. T.; Griffin, R. J.; Guyenne, S.; Hutton, C.; Kaellblad, P.; Kemp, S. J.; Kitching, M. S.; Newell, D. R.; Norbedo, S.; Northen, J. S.; Reid, R. J.; Saravanan, K.; Willems, H. M. G; Lunec, J.J. Med. Chem. 2006, 49, 6209-6221.
  • 9Shen, R.; Huang, X. J. Org. Chem, 2007, 72, 3961-3964.
  • 10For Preparation of TsNBr2, See: Hair, C. G R.; Indrasen, P. Talanta 1976, 23, 239.

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部