苯甲醛缩氨基硫脲Fe(Ⅱ)、Sn(Ⅱ)配合物的直接电化学合成

Direct electrochemical synthesis of Fe(Ⅱ)， Sn(Ⅱ) with benzaldehyde thiosemicarbazone complexes

用电化学金属阳极氧化法在非水溶剂中合成了苯甲醛缩氨基硫脲（ Ｈ Ｌ）与 Ｆｅ（Ⅱ）、 Ｓｎ（Ⅱ）配合物，通过元素分析、红外光谱、紫外光谱、磁矩、摩尔电导等对配合物进行了表征。

Fe(Ⅱ), Sn(Ⅱ) with benzaldehyde thiosemicarbazone complexes are synthesized by the electrochemical oxidation of anodic metal in non aqueous solvent. The complexes are characterized with elemental analysis, IR, UV, magnetic measurement, and molar conductivity.\;