摘要
A silicone oil emulsion with 60% of solid content was prepared with methyl silicone oil used as the main material by means of the emulsifier-in-oil method.The influence of emulsification conditions on the droplet diameter of silicone oil emulsion was discussed.The experimental results showed that the emulsification method,including the quantity of the emulsifier,the time and temperature of emulsification,the emulsifying water dosage,and the stirring speed,had significant impact on the droplet size.The optimal conditions were identified to achieve a smallest droplet diameter of the emulsion at an emulsifier dosage of 6%,an emulsification temperature of 70 ℃,an emulsification time of 30 min,and a stirring speed of 1100 r/min,with water added in two portions at a ratio of 1:1.The high-solid content silicone oil emulsion with a mean droplet diameter of 2.731 μm was prepared under these conditions that could ensure absence of stratification and floating oil under centrifuging at a speed of 3000 r/min for 30 min.
A silicone oil emulsion with 60% of solid content was prepared with methyl silicone oil used as the main material by means of the emulsifier-in-oil method. The influence of emulsification conditions on the droplet diameter of silicone oil emulsion was discussed. The experimental results showed that the emulsification method, including the quantity of the emulsifier, the time and temperature of emulsification, the emulsifying water dosage, and the stirring speed, had significant impact on the droplet size. The optimal conditions were identified to achieve a smallest droplet diameter of the emulsion at an emulsifier dosage of 6%, an emulsification temperature of 70 ℃, an emulsification time of 30 min, and a stirring speed of 1100 r/min, with water added in two portions at a ratio of 1：1. The high-solid content silicone oil emulsion with a mean droplet diameter of 2.731 μm was prepared under these conditions that could ensure absence of stratification and floating oil under centrifuging at a speed of 3000 r/min for 30 min.
