7-氨基-4,6-二硝基苯并氧化呋咱的合成反应研究

On the synthesis of 7-amino-4,6-dinitrobenzofuroxan

分析和讨论了以3-氯苯胺为原料,经酰化、硝化、叠氮化热解脱氮及水解合成7-氨基-4,6-二硝基苯并氧化呋咱反应的机理及反应条件.此反应收率高,条件温和.

The synthesis is discussed of compound 7-amino-4, 6-dinitrobenzofuroxan, via acylation, ni- tration, azidation/pyrolysis-denitrogenation and hydrolysis. The yield is high and condition mild.