摘要
The effect of cold plastic deformation between solution treatment and artificial aging on the age-hardening response and mechanical properties of alloy was investigated by micro-hardness test,tensile test,optical microscopy(OM) and TEM observation.After solution treatment at 420 ℃ for 1 h,three kinds of pre-deformation strains,i.e.0,5% and 10%,were applied to extruded ZM61 bars.Age-hardening curves show that pre-deformation can significantly accelerate the precipitation kinetics and increase peak-hardness value;however,as pre-deformation strain rises from 5% to 10%,there is no gain in peak hardness value.The room temperature(RT) tensile properties demonstrate that increasing the pre-deformation degree can enhance the yield strength(YS) and ultimate tensile strength(UTS) but moderately reduce elongation(EL);furthermore,the enhancement of YS is larger than that of UTS.No twin can be observed in 5% pre-deformed microstructure;however,a large number of twins are activated after 10% pre-deformation.The peak-aged TEM microstructure shows that pre-deformation can increase the number density of rod-shaped β 1 ' precipitates which play a key role in strengthening ZM61 alloy.
采用显微硬度测试、拉伸试验、金相观察和TEM观察,研究冷塑性变形对Mg-6%Zn-1%Mn(ZM61)合金时效硬化和力学性能的影响。在420℃固溶处理1h后,对ZM61挤压棒材试样进行室温拉伸变形,塑性应变有3种:0、5%和10%,预变形后再进行人工时效。时效硬化曲线表明:预变形可以显著加快硬化速率且提高峰值硬度;然而,当应变量由5%增加到10%后,峰值硬度并未增加。室温拉伸性能表明:预变形量增加,屈服强度和抗拉强度增加,伸长率略有降低,且屈服强度的增加幅度大于抗拉强度的。金相组织观察表明:当预变形应变量为5%时,金相组织中未观察到孪晶;预变形10%的组织中出现了大量的孪晶。TEM观察表明:预变形可以增加峰时效态组织中β1′杆状相的数量。
基金
Project(2007CB613700) supported by the National Basic Research Program of China
Project(50725413) supported by the National Natural Science Foundation of China
Project(CDJXS11132228) supported by the Fundamental Research Funds for the Central Universities,China
Projects(2010DFR50010,2008DFR50040) supported by International Cooperation Program,China
Projects (CSTC2009AB4008,2010CSTC-HDLS) supported by Chongqing Sci & Tech Program,China