摘要
用水热方法合成了 (phen)Fe(H2 O)Cl3晶体 ,并用X—射线衍射对其结构进行了表征 .该晶体属于三斜晶系 ,P -1空间群 ,a =6.61 9(1 ) ,b=1 0 .2 3 1 (2 ) ,c=1 0 .60 6(2 ) ,α=92 .0 78(1 9)°,β=1 0 0 .661 (1 4)° ,γ =1 0 8.1 88(1 1 )°,v=667.2 (2 ) 3。
A crystal of (phen)Fe(H 2O)Cl 3 has been synthesizde by the hydrothermal method and characterizated by X-ray structure diffraction.Crystal data for the title compound,monoclinic,space group P -1 with a =6.619(1)?, b =10.231(2)?, c =10.606(2)?,α=92.078(19)°,β=100.661(14)°,γ=108.188(11)°, v =667.2(2)? 3, z =2.
出处
《松辽学刊(自然科学版)》
2002年第2期62-64,共3页
Songliao Journal (Natural Science Edition)
基金
吉林省教委基金 [0 0 47]
山东大学晶体材料国家重点实验室开放基金资助 [0 0 10 ]