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The Synthesis of Cyclic Amino Acids 被引量：2

The Synthesis of Cyclic Amino Acids
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摘要 Several cyclic amino acids (1-4) were synthesized from glycine. Isocyanate ester was prepared as the key intermediate and reacted with dibromoalkanes to afford the target compounds. Several cyclic amino acids (1-4) were synthesized from glycine. Isocyanate ester was prepared as the key intermediate and reacted with dibromoalkanes to afford the target compounds.
作者 Shrong Shi LIN
机构地区 College of Chemical and Molecular Engineering
出处 《Chinese Chemical Letters》 SCIE CAS CSCD 2003年第9期883-884,共2页 中国化学快报（英文版）
基金 the National Natural Science Foundation of China(No.20272001)
关键词 Cyclic amino acid isocyanate ester dibromoalkane ion exchange resin. Cyclic amino acid, isocyanate ester, dibromoalkane, ion exchange resin.
分类号 O624 [理学—有机化学]
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参考文献3

  • 1D. O. Adams, S. F. Yang, Proc. Natl. Acad. Sci.. USA. 1979. 76. 170.
  • 2D. Kalvin, K. Ramalingam, R. W. Woodard, Synth. Comm., 1985, 15, 267.
  • 31H NMR (300 MHz, in D2O if not specified, δppm) of 1: 1.27 (m, 2H, CH2), 1.37 (m, 2H,CH2). IH NMR of2:1.40 (m, 2H, CH3), 1.73 (t, 4H, J= 5.5 Hz, CH2). 1H NMR of 3:1.65 (t,4H, J = 8.0 Hz, CH2), 1.95 (t, 4H, J=7.5 Hz, CH2); 1H NMR of 4:1.25 (t, 2H, J = 8.5 Hz,CH2), 1.60 (m, 4H, CH2). 1.90 (t, 4H, J=10 Hz, 4H); 1H NMR (CDCl3) of 6: 1.29 (t, 3H, J =6.SHz, CH3), 4.07 (d, 2H, J = 5.4Hz, CH2), 4.23 (q, 2H, J = 7.0Hz, CH2), 6.85 (s, 1H, NH),8.26 (s, 1H, CHO). 1H NMR (CDCl3) of 7: 1.32 (t, 3H, J = 7.4 Hz, CH3), 4.24 (s, 2H, CH2),4.29 (q, 2H, J = 7.4 Hz, CH2). 1H NMR (CDCI3) of 8:1.30 (t, 3H, J = 7.2Hz, CH3),1.53-1.61 (m, 4H, CH2CH2), 4.23 (q, 2H, J = 7.0 Hz, CH2). 1H NMR (CDCl3) of9: 1.32 (t,3H, J=7.2Hz, CH3), 1.90 (t, 2H, CH2), 2.10 (t, 4H, J=10Hz, CH2), 4.25 (q, 2H, J = 7.0 Hz,CH2).

同被引文献8

  • 1Douglas K, Kondareddiar R, Ronald W. A facile procedure for the preparation of alicyclic a-amino acids [ J ]. Synth Comm, 1985,15:267 - 272.
  • 2张本田,赵传江.甘氨酸乙酯盐酸盐的生产方法[P].CN1733705A,2006,2:15.
  • 3Adama D O,Yang S F.Ethylene biosynthesis:Identification of 1-aminocyclopropane-1-carboxylic acid as an intermediate in the conversion of methionine to ethylene[J].Proc Natl Acad Sci,1979,76:170-174.
  • 4Yang S F,Hoffman N E.Ethylene biosynthesis and its regulation in higher plants[J].Annu Rev Plant Physiol,1984,35:155-189.
  • 5Pirrung MC.Ethylene biosynthesis from 1-aminocyclopropanecarboxylic acid[J].Acc Chem Res,1999,32:711-718.
  • 6Hartman G D,Weinstock L M.Thiazoles from ethyl isocyanoacetate and thiono esters:ethyl thiazole-4-carboxylate[J].Organic Syntheses,1979,59:183-188.
  • 7Douglas K,Kondareddiar R,Ronald W.A facile procedure for the preparation of alicyclic α-amino acids[J].Synth.Comm,1985,15:267-272.
  • 8李能刚,王超志,刘炳朋,吴晓明.2-正丁基-1,3-二氮杂螺[4,4]壬-1-烯-4-酮的合成[J].中国新药杂志,2002,11(6):467-468. 被引量：1

引证文献2

Chinese Chemical Letters
2003年 第9期

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