摘要
In nuclear industry,the purity of hafnium control rod is usually significant,and the process parameters will affect the impurity contents.In this study,the four key factors(filament temperature,retort materials,feeds,and iodide reaction time)were investigated.It is found that the impurity contents of Fe,Ni in the hafnium crystal bar decrease with the K value rising.Both the retort materials and feed types have obvious influence on the impurity contents of hafnium crystal bar.The iodide reaction time has little effect on the impurity contents of hafnium crystal bar.
In nuclear industry,the purity of hafnium control rod is usually significant,and the process parameters will affect the impurity contents.In this study,the four key factors(filament temperature,retort materials,feeds,and iodide reaction time) were investigated.It is found that the impurity contents of Fe,Ni in the hafnium crystal bar decrease with the K value rising.Both the retort materials and feed types have obvious influence on the impurity contents of hafnium crystal bar.The iodide reaction time has little effect on the impurity contents of hafnium crystal bar.
基金
financially supported by the National Technology Support Project of China(No.2012BAB10B10)
the China-Russia Corporation Program Ministry of Science(No.2010DFR50800).