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pH值对胶体金制备的影响 被引量:8

Influence of pH on Preparation of Colloidal Gold
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摘要 研究了不同的溶液pH值对胶体金颜色、粒径的影响。在不同pH值下通过柠檬酸三钠法制备胶体金溶液,利用紫外/可见光吸收分光光度计对胶体金进行扫描,得到最大吸收峰波长及峰宽;通过透射电镜观察其颗粒直径及分布,再将二者结果进行比较分析。结果显示:随着溶液pH值变小,胶体金颜色由红→蓝→黑,粒径变大。 The color and the particle size of colloidal gold were influenced by different pH values. Colloidal gold was prepared with sodium citrate by controlling the pH of the solution. The maximum of absorption and its peak width were obtained from UV/visible absorption spectrophotometry. The diameter and its distribution were measured by transmission electron microscopy (TEM). Then the results were compared and analyzed. The result shows that with the decrease of the pH, the particle size increases and the color o...
出处 《稀有金属》 EI CAS CSCD 北大核心 2005年第4期468-470,共3页 Chinese Journal of Rare Metals
关键词 胶体金 PH值 粒径 柠檬酸三钠法 colloidal gold pH values particle size sodium citrate
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  • 2[3]Frens G. Controlled nucleation for the regulation of the particle size in monodisperse gold suspensions [J]. Nat.Phys. Sci., 1973, 241(105): 20.
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  • 4杨振修,陈宪莲,陶义训.银强化金标记免疫吸附剂试验的方法学研究[J].上海免疫学杂志,1996,16(1):42-43. 被引量:40

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