摘要
将环状低聚糖α-环糊精(α-CD)应用于薄层色谱,以国产聚酰胺膜为固定相,研究了同分异构体邻、间、对苯二酚的薄层色谱行为及影响分离的因素;建立了苯二酚异构体的分析方法;探讨了苯二酚化合物与α-CD的键合常数,并提出了可能的包接模型.
The use of aqueous solution of α-cyclodextrin as the mobile phase in TLC was described. The chromatographic characteristics of ortho, meta and para substituted hydroxyphenol are investigated by using polyamide membrane as the fixed phase. The factors affecting separation are discussed in detail. The analytical method for the substituted hydroxyphenol isomers has been established. The equilibrium binding constants of inclusion complex are determined and possible inclusion model were proposed.
出处
《华南理工大学学报（自然科学版）》
EI
CAS
CSCD
北大核心
1997年第11期13-16,共4页
Journal of South China University of Technology(Natural Science Edition)
基金
山西省留学回国人员基金资助项目
关键词
Α-环糊精
薄层色谱
羟基苯酚
α-cyclodextrin
thin layer chromatography
hydroxyphenol
