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分光光度法测定食品中微量铅 被引量:3

Determination of Trace Element of Lead in Food
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摘要 研究邻硝基苯基荧光酮(O—NPF) —溴代十六烷基三甲铵(CTMAB) —铅(Pb) 体系测定微量铅。研究表明,该方法灵敏度高,稳定性好,测定简便快速,其表观摩尔吸光系数为2-13·105 L·mol- 1·cm - 1 ,比耳定律适用范围为0 ~25 μg/50 m L,适用于食品、污水中微量铅的测定。 Trace element lead which reacts with orthonitrobenzfluorenone in the presence of cetyl trimethylammonium bromide was studied. The proposed method is proved to be sensitive, stable, rapid and convenient. The apparent molar absorbtivity is 2.13·10 5 L·mol -1 ·cm -1 . Beer's valid within the range of 0~25 μg/50 mL. The method is applicable the direct determination of lead in food and waste water.
出处 《安徽机电学院学报》 1999年第4期52-55,共4页 Journal of Anhui Institute of Mechanical and Electrical Engineering
关键词 光度法 测定 食品 spectrum analysis determination food lead
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同被引文献25

  • 1袁建,鞠兴荣,汪海峰,沈崇钰,蒋原.茶叶中有害金属元素的快速检测技术研究[J].食品科学,2004,25(11):259-263. 被引量:18
  • 2李新华.示差脉冲溶出伏安法测定食盐中痕量铅[J].理化检验(化学分册),2005,41(2):119-120. 被引量:10
  • 3石元值,康孟利,马立锋,韩文炎.茶园土壤中铅形态的连续浸提测定方法研究[J].茶叶科学,2005,25(1):23-29. 被引量:22
  • 4陈天金,魏益民,潘家荣.食品中铅对人体危害的风险评估[J].中国食物与营养,2007,13(2):15-18. 被引量:72
  • 5Poliana Carolina Aleixo, Dario Santos Junior, Andrea Cristina Tomazelli ,et al. Cadmium and lead determineation in foods by beam injection flame furnace atomic absorption spectrometry after ultrasoundassisted sample preparation [ J ]. Analytica Chimica Acta, 2004 (512) :329 -337.
  • 6Drake P L, Lawryk N J. Ev-aluation of two portable lead-monitoring methods at mining sites[ J]. Journal of Hazardous Materials, 2003 ( 102 ) :29 -38.
  • 7Eric Fischer, Constant M G, Van den Berg. Anodic stripping voltammetry of lead and cadmium using a mercury film electrode and thiocyanate[ J ]. Analytica Chimica Acta, 1999,385 ( 1 - 3 ) : 273 -280.
  • 8Slavka Stankovic, Dragana Cickaric, Jelena Markovic. Determination of Pb and Cd in water by potentiometric stripping analysis (PSA) [ J ]. Desali-nation,2007,213 ( 1 -3 ) :282 -287.
  • 9Shams E, Abdollahi H, Yekehtaz M, et al. H-point standard addition method in the analysis by differential pulse anodic stripping vohammetry : Simultaneous determination of lead and tin [ J ]. Talanta,2004 ,63 (2,28) :359 -364.
  • 10GB/T500912-2003,食品中铅的测定[S].

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