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壳聚糖席夫碱钯配合物的合成与表征 被引量：3

Synthesis and Characterization of Chitosan Schiff-base Palladium Complex
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摘要 用水杨醛改性后的壳聚糖席夫碱与PdCl2反应得到壳聚糖席夫碱钯配合物.壳聚糖、壳聚糖席夫碱及其钯配合物用红外光谱(IR)、X-射线光电子能谱(XPS)、X-射线衍射光谱(XRD)、热分析(TG-DTA)以及荧光光谱等分析手段进行了表征分析,根据表征结果提出了壳聚糖席夫碱钯配合物的可能结构. Chitosan schiff-base palladium complex is synthesized from the reaction of chitosan schiff-base formed by salicylaldehyde via grafting and palladium chloride.The structure of chitosan,schiff-base and chitosan schiff-base palladium complex are characterized by IR,XPS,XRD,TG-DTA and fluorescence,according to the results of analysis,the structure of chitosan schiff-base palladium complex can be inferred.
作者 张鹏 杨光瑞 刘蒲
机构地区 华北水利水电学院 郑州大学化学系
出处 《华北水利水电学院学报》 2008年第3期71-73,共3页 North China Institute of Water Conservancy and Hydroelectric Power
关键词 壳聚糖 席夫碱 钯配合物 IR XPS XRD TG-DTA 荧光光谱 chitosan schiff-base palladium complex IR XPS XRD TG-DTA fluorescence
分类号 O641.4 [理学—物理化学]
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华北水利水电学院学报
2008年 第3期

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