摘要
介绍了以2,6-二氯甲苯为原料,经醚化、格氏反应、水解三步反应合成3-甲氧基-2-甲基苯甲酸的合成工艺。合成总收率达到72%,产品纯度达到99%。
methoxy-2-methylbenzoic acid was synthesized from 2,6-dichlorotoluene by methoxylation, Grignard reaction and hydrolization, its total yield and purity is 72%,99.1% respectively.
出处
《广东化工》
CAS
2004年第9期-,共2页
Guangdong Chemical Industry