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表面活性剂辅助水热法制备ZnS纳米线 被引量:1

Hydrothermal Synthesis of Nanowires ZnS with Surfactant
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摘要 用十二烷基硫醇做表面活性剂,用水热法在180℃,12 h条件下制备了ZnS纳米线.实验发现硫醇可以诱导ZnS纳米粒子沿着一维方向生长.所得产物ZnS纳米线为六方纤锌矿结构,直径为50 nm~100 nm,长度10 μm~20 μm.用X射线衍射(XRD)、透射电子显微镜(TEM)、扫描电子显微镜(SEM)、荧光发射光谱(PL)和紫外漫反射光谱(UV)等手段对所得纳米线进行了表征,并初步探讨了硫醇在限制ZnS纳米晶一维方向生长的机理.
机构地区 浙江大学
出处 《稀有金属材料与工程》 SCIE EI CAS CSCD 北大核心 2004年第z1期239-241,共3页 Rare Metal Materials and Engineering
基金 国家教育部"跨世纪人才"及国家自然科学基金委员会资助(69890230).
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同被引文献19

  • 1裴立宅,唐元洪,郭池,陈扬文,张勇.水热法及溶剂热合成法制备Ⅳ族一维无机纳米材料[J].稀有金属,2005,29(2):194-199. 被引量:15
  • 2WANG X J, WAN F Q, HAN K, et al. Large - scale synthesis well - dispersed ZnS microspheres and their photoluminescence,photocatalysis properties [ J ]. Materials Characterization,2008,59:1765 - 1770.
  • 3PANDA SK, CHAUDHURI S. Chelating ligand - mediated synthesis of hollow ZnS microspheres and its optical properties [ J ]. J Colloid and Interface Sci ,2007,313 ( 1 ) :338 - 344.
  • 4CHANG L J,WANG Q Z,GUI F Z,et al. Hydrothermal synthesis and characterization of ZnS microspheres and hollow nanospheres [ J ]. Materials Chemistry and Physics ,2007,103:24-27.
  • 5CHENG C W, XU G Y, ZHANG H Q, et al. Low-temperature synthel sis and optical properties of wurtzite ZnS nanowires[J]. Materials Let- ters,2006,60:3561 - 3564.
  • 6MASOUD S N, MOHAMMAD R L E, FATEMEH D. Controllable synthesis of wurtzite ZnS nanorods through simple hydrothermal method in the presence of thioglycolic acid [ J ]. Journal of Alloys and Compounds ,2009,475:782 - 788.
  • 7WEI F, LI G C, ZHANG Z K. Hydrothermal synthesis of spindle - like ZnS hollow nanostructures [ J ]. Materials Research Bulletin,2005,40 : 1402 - 1407.
  • 8ZHANG Y C, WANG G Y, HU X Y. Solvothermal synthesis of uniform hexagonal - phase ZnS nanorods using a single - source molecular precursor[ J ]. Materials Research Bulletin,2006,41 : 1817 - 1824.
  • 9ZHAO Q T,HOU L S,HUANG R A. Synthesis of ZnS nanorods by a surfactant - assisted soft chemistry method [ J ]. Inorganic Chemistry Communications ,2003,6:971 - 973.
  • 10常鹏,刘肃,王秀华,唐莹.水热法制备硫化锌纳米线及性能研究[J].人工晶体学报,2007,36(4):817-820. 被引量:12

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