有机液、消毒液中相关化合物的GC-MSD分析测定

Analysis of Relative Compounds in Organic and Decon Samples by GC - MSD

禁止化武公约组织(OPCW)每年都要考核各参试国家的分析能力,我们实验室连续多年参加水平考试,并都取得了很好的成绩.本文报导了第14次OPCW水平考试其中的有机液(O/14)和消毒液(D/14)样品分析.有机液是模拟视查某生产、合成车间,采自1个未作标记包装容器内的样品(编号O/14).……

The fourteenth official OPCW proficiency test organic sample and Decon sample were analyzed by GC-MSD. There were a lot of impurities in the organic sample. Relative compounds were not separated by DBS-MS column, but DB-1701 chromatography column can separate them. Organic sample was extracted by acetonitrile to remove background. The Decon sample was extracted by dichloromethane. All compounds in two samples were determined successfully.