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溶胶-共沸蒸馏与凝胶-共沸蒸馏制备8YSZ纳米粉体对烧结性能的影响 被引量:1

Influence of Sol- and Gel- Azeotropic Distillation Methods on the Sinterability of 8YSZ Nanometer Powder
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摘要 本文采用溶胶-共沸蒸馏和凝胶-共沸蒸馏制备法出了一次粒径<10 nm的8YSZ(Y2O3稳定的立方ZrO2.Y2O3摩尔含量8%)粉体.产物采用XRD,BET,FTIR和TG/DSC等手段进行了表征.粉体经分散后采用浸渍提拉的方法在多孔LSM(锰酸镧锶)基片上涂膜.薄膜的烧结实验表明:采用溶胶-共沸蒸馏制备的粉体烧结活性很高,在1200℃下烧结就实现了完全致密化;而采用凝胶-共沸蒸馏制备的粉体烧结活性很差,1300℃下10 h仍未能烧结.造成这种差别的主要原因是凝胶-共沸蒸馏制得的粉体存在着严重的硬团聚,文中对硬团聚产生的原因和机理进行了探讨,并提出了一种避免硬团聚的方法.
出处 《过程工程学报》 CAS CSCD 北大核心 2004年第z1期515-520,共6页 The Chinese Journal of Process Engineering
基金 863基金项目,编号为:2003AA323010
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