Reductive Coupling of Alkyl Selenocyanates to Diselenides Utilizing Environmentally Benign TiCl4-NEt3 Reagent

Reductive Coupling of Alkyl Selenocyanates to Diselenides Utilizing Environmentally Benign TiCl4-NEt3 Reagent

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摘要　　The reduction of TiCl4 to low valent titanium (LVT) species and the synthetic utility of such species are welldocumented chemistry of wide interest. [1] Generally, reducing agents such as Mg, Zn, Li, Sm, Pb-Te and LiAlH4are used for reduction of TiCl4.[2]……

作者 HUANG You FENG De-Xin CHEN Ru-Yu

机构地区 Institute and State Key Laboratory of Elemento-Organic Chemistry

出处《有机化学》 SCIE CAS CSCD 北大核心 2003年第z1期164-164,共1页 Chinese Journal of Organic Chemistry

分类号 O62 [理学—有机化学]

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1[1]Mccmurry, J. E. Chem. Rev. 1989, 89, 1513.
2[2]Fürstner, A.; Bogdanovic, B. Angew. Chem., Int. Ed. Engl. 1996, 35, 2442.

1Wei Xing QIAN(Medical Chemistry Division,Zhejiang Medical University, Hangzhou, 310006) Wei Liang BAO,Yong Min ZHANG(Department of Chemistry,Hangzhou University, Zhejiang, 310028).Synthesis of α-Selenoesters By Reactions of α-Bromoesters With Diselenides Promoted By Metallic Tin[J].Chinese Chemical Letters,1997,8(8):681-682.
2许孝良,张永敏.Synthesis of the Cyclopentenylamine Derivatives Promoted by SmI_2[J].Chinese Journal of Chemistry,2003,21(1):98-100.
3Barahman Movassagh,Mona Moradi.One-pot synthesis of selenocarbamates from isocyanates and diselenides using the Zn/AlCl_3 system[J].Chinese Chemical Letters,2013,24(3):192-194.
4Zhi Fang LI,Ping LU,Yong Min ZHANG(Department of Chemistry, Zhejiang University (Xixi campus), Hangzhou 310028Laboratory of Organometallic Chemistry, Institute of Organic Chemistry Chinese Academy of Sciences, Shanghai 200032).Facile Synthesis of Amidines via Intermolecular Reductive Coupling of Nitriles with Azobenzene Promoted by Samarium Diiodide[J].Chinese Chemical Letters,2000,11(6):495-498. 被引量：1
5张纪明,张永敏.Reductive Coupling Cyclization of 1,1-Dicyanoalkenes Promoted by Sm^0/cat. HgCl_2 System[J].Chinese Journal of Chemistry,2002,20(7):688-691.
6JiMingZHANG,YongMinZHANG.Catalytic HgCl_2-Samarium System Induced Reductive Coupling of Nitriles with Nitro Compounds[J].Chinese Chemical Letters,2002,13(2):97-100.
7TAYEBEE, Reza,ALIZADEH, Mohammad Hassan.Environmentally Benign Oxidation of Some Organic Sulfides with 34% Hydrogen Peroxide Catalyzed by Simple Heteropolyoxometalates[J].Chinese Journal of Chemistry,2007,25(9):1340-1343. 被引量：1
8LIUXiaozhi PENGAidong LUShiwei.An Environmentally Benign Method for Preparation of Nitroanilines[J].催化学报,2003,24(10):731-732. 被引量：1
9Hong-Wei Shi,Chen Yu,Jie Yan.Potassium bromide or sodium chloride catalyzed acetoxyselenenylation of alkenes with diselenides and mCPBA[J].Chinese Chemical Letters,2015,26(9):1117-1120.
10Wei Xing CHEN,Jian Xie CHEN,Jian Ping JIANG,Tsi Yu KAO.LOW-VALENT TITANIUM INDUCED REDUCTIVE COUPLING OF AROMATIC NTTRILES TO 1,2-ARYLETHANONES[J].Chinese Chemical Letters,1991,2(5):351-352.

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Reductive Coupling of Alkyl Selenocyanates to Diselenides Utilizing Environmentally Benign TiCl4-NEt3 Reagent

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