期刊文献+

利用TRPO-煤油/盐酸-ZrOCl_2萃取体系的第三相制备ZrO_2介孔材料

Preparation of Mesoporous ZrO_2 With the Middle Phase Formed in TRPO-Kerosene/HCl-ZrOCl_2 Extraction System
下载PDF
导出
摘要 首次利用TRPO-煤油/HCl-Zr(Ⅳ)萃取体系中负载Zr(Ⅳ)的第三相作为模板和Zr(Ⅳ)源,采用冷冻的方法成功地制备了ZrO2介孔材料。并利用TG-DTA,TEM,XRD,N2吸附-脱附等方法对所制得的材料进行表征。 The third phase formed in TRPO-kerosene/ HCl-ZrOCl2extraction system is first used as both Zr(Ⅳ)source and the template to prepare mesoporous ZrO2 just by precipitation with aqua ammonia under low temperature . TG-DTA, TEM, XRD and N2 adsorption-desorption are adopted for the characterization of the synthesized sample.
作者 尹德成
出处 《现代技术陶瓷》 CAS 2008年第2期28-31,共4页 Advanced Ceramics
关键词 TRPO 第三相 ZRO2 介孔材料 TRPO the third phase ZrO2 msoporous material
  • 相关文献

参考文献6

  • 1Hudson MJ,Knowles J A.Preparation and characteriza-tion mesoporous,high surface area zirconium(Ⅳ)ox-ides[].Journal of the American Chemical Society.1995
  • 2Huang Y,Sachtler W M H.Preparation of mesostruc-tured lamellar zirconia[].J Chem Soc Chem.1997
  • 3Ulagappan N,N,Battaram V N,et al.Preparation of la-mellar and hexagonal forms of mesoporous silica and zir-conia by the neutral amine route:lamellar-hexagonal transformation in the solid state[].Chemical Communications.1996
  • 4Kim A,Bruinsma P,Chen Y,et al.Amphoteric surfac-tant templating route for mesoporous zirconia[].Chemical Communications.1997
  • 5YANG, CF,CHEN, JY.Electron Microscopy Studies on Ultrafine Zirconia Powders from Solvent Extraction with Tributyl Phosphate in Kerosene[J].Journal of Materials Science & Technology,1995,11(3):217-221. 被引量:2
  • 6Shi J,Gu G,Fu X,et al.Extraction behavior and phase behavior of TOPO(or TRPO)-Kerosene/Ti(Ⅳ)-H2SO4systems and the preparation of TiO2by predisper-sed-hydrolytic method[].Colloids and Surfaces.2001

共引文献1

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部