2-(2-苯胺乙基)吡啶的合成和晶体结构

Synthesis and Crystal Structure of 2-(2-anilinoethyl)-Pyridine

本文合成了2-(2-苯胺乙基)吡啶并用X-射线衍射法测定了其晶体结构。该分子以正交空间群Pbca结晶,晶胞参数为a=7.1899(2),b=14.6317(3),C=21.6144(1) ,D_(calc)1.158 g cm^(-1),Z=8。在晶体中,分子间通过N—H…N氢键沿a轴排列成链状。

The title compound has been synthesized and its crystal structure determined by X-ray diffraction meth- ods. It crystallizes in the orthorhombic space group Pbca, with a=7. 1899(2), b=14. 6317(3), c=21. 6144(1) , and D_(calc)=1. 158g cm^(-1) for Z=8. In the structure, the molecules are arranged as chains running along the a axis through N-H…N hydrogen bonds.