1—环己胺基蒽醌的合成

Synthesis of 1-Cyclohexylamino-9,10-Anthracenedione

以1-氯蒽醌和环己胺为原料合成1-环己胺基蒽醌,研究了化学反应的影响因素,得出了佳化工艺条件:反应温度120℃,反应时间8h,产品纯度大于98.5%,产品收率大于97%。

The synthesis of 1-cyclohexylamino-9,10-anthracenedione was prepared by reaction of cyclohexylamine with 1-chloroanthracenedione. A study of the effects on the synthesis was done. The reaction conditions recommended were as follows:reaction time was 8 h,reaction temperature was 120 ℃. The yield was over 97%,and the purity was over 98.5%.