摘要
以苯胺为原料,用冰醋酸和醋酸作乙酰化剂,经乙酰化、硝化、还原合成了对氨基乙酰苯胺。还原温度(98±1)℃,还原液pH=5.1~5.5,产品收率达70%左右。
p-Aminoacetanilide was synthesized by the acetyization of aniline with acetic acid and acetic anhydride, then nitration and reduction. Reduction temperature was 98±1℃, pH=5.1-5.5. The yield of product was about 70%.
出处
《染料与染色》
CAS
2001年第6期42-43,共2页
Dyestuffs and Coloration
关键词
苯胺
乙酰化
硝化
对氨基乙酰苯胺
aniline acetylization nitration p-aminoacetanilide