Determination of Enantiomeric Purity of ν-Pyrrolidinyl Phenylpropanol by Capillary Electrophoresis Using β-Cyclodextrin Polymer as Chiral Selector
Determination of Enantiomeric Purity of ν-Pyrrolidinyl Phenylpropanol by Capillary Electrophoresis Using β-Cyclodextrin Polymer as Chiral Selector
摘要
Enantiomer of n-pyrrolidinyl phenylpropanol was studied by capillary electrophoresis using b-cyclodextrin polymer as chiral selector. We determined the enantiomeric excess value of n-pyrrolidinyl phenylpropanol with RSD 0.48%.
Enantiomer of (-pyrrolidinyl phenylpropanol was studied by capillary electrophoresis using (-cyclodextrin polymer as chiral selector. We determined the enantiomeric excess value of (-pyrrolidinyl phenylpropanol with RSD 0.48%.
-
1ZHANG Da-tong,TANG Li-da,DUAN Gui-yun,ZHAO Gui-long,XU Wei-ren,MENG Li-juan,WANG Jian-wu.Synthesis, Resolution, and Enantiomeric Purity Assay of 2-n-Butylbutanedioic Acid 4-t-Butyl Esters[J].Chemical Research in Chinese Universities,2006,22(5):584-588.
-
2Xin Rong QIN,Quan LI,Yu Yuan XIE.Synthesis of (s)-(-)-Benzyl-2-tert-butoxycarbonyl amino-4-iodobutyrate[J].Chinese Chemical Letters,2001,12(9):767-768. 被引量:1
-
3吴文连,吴毓林.糖作为EPC合成手性源[J].化学进展,1993,5(2):67-81.
-
4Bruno Gallinella,Rosella Ferretti,Leo Zanitti,Isabella Sestili,Antonina Mosca,Roberto Cirilli.Comparison of reversed-phase enantioselective HPLC methods for determining the enantiomeric purity of (S)-omeprazole in the presence of its related substances[J].Journal of Pharmaceutical Analysis,2016,6(2):132-136. 被引量:2
-
5蒋晟,吴毓林,姚祝军.First Synthesis of Mosquito Larvicidal Butenolides I and II[J].Chinese Journal of Chemistry,2002,20(7):692-696.