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溶剂热还原合成Cr_2O_3纳米管(英文) 被引量:17

A Solvothermal-reduction Approach to Crystalline Cr_2O_3 Nanotubes Synthesis
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摘要 Cr2O3 nanotubes with diameters of 80 nm and lengths of 550 nm were synthesized in a solvothermal reduction system at 180 ℃. The acetyl acetone (AcAc) and ethylene glycol (EG) were used as the chelate agent and the reductant respectively in the system. An intermediate compound-Cr(C5H7O2)3 was formed to force Cr2O3 to crystallize along one direction. Cr2O3 nanotubes with diameters of 80 nm and lengths of 550 nm were synthesized in a solvothermal reduction system at 180 degreesC. The acetyl acetone (AcAc) and ethylene glycol (EG) were used as the chelate, agent and the reductant respectively in the system. An intermediate compound-Cr(III)(C5H7O2), was formed to force Cr2O3 to crystallize along one direction.
出处 《无机化学学报》 SCIE CAS CSCD 北大核心 2004年第8期971-974,共4页 Chinese Journal of Inorganic Chemistry
基金 国家自然科学基金资助项目(No.20125103 90206034)。
关键词 三氧化二铬纳米管 溶剂热还原 合成 乙酰丙酮 乙二醇 solvothermal reduction acetyl acetone ethylene glycol Cr (III) oxide nanotubes
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