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苯亚磺酸与环氧乙烷合成2-(苯基磺酰基)乙醇过程中副产物分析 被引量:2

An Analysis on By-products of 2-(Phenylsulfonyl) ethanol Synthesized from Benzenesulfinic Acid and Ethylene Oxide
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摘要 2-(苯基磺酰基)乙醇可由苯亚磺酸和环氧乙烷合成,本文对反应中出现的两个副产物经核磁、红外、质谱表征,确定了其结构。分析了产生途径,并进行了合成验证,对副产物的回收利用方法进行了探讨。 2-(Phenylsulfonyl)ethanol could be synthesized from benzenesulfinic acid and ethylene oxide,The chemical structures of two by-products of the reaction were characterized by NMR,IR and MS. Possible synthesis routes of two by-products were analyzed and they were confirmed by synthesis,the reclamation of by-products were studied.
出处 《染料与染色》 CAS 2012年第2期54-57,38,共5页 Dyestuffs and Coloration
关键词 染料中间体 2-(苯基磺酰基)乙醇 副产物分析 结构表征 dye intermediates 2-(phenylsulfonyl)ethanol by-products analysis structure characterization
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