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Synthesis of a novel benzoxazine containing benzoxazole structure 被引量：4

Synthesis of a novel benzoxazine containing benzoxazole structure
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摘要 A high-purity benzoxazine（Boz-BOA） containing benzoxazole structure was successfully synthesized by three-step synthetic method using 2-（4-aminophenyl）-1H-benzoxazole-5-amine（BOA） and ortho-hydroxybenzaldehyde.The structure of Boz-BOA was confirmed by FTIR and;H NMR spectra.The DSC was utilized to probe the curing behavior of Boz-BOA and exhibited a narrow melting peak and curing exothermic peak. A high-purity benzoxazine(Boz-BOA) containing benzoxazole structure was successfully synthesized by three-step synthetic method using 2-(4-aminophenyl)-1H-benzoxazole-5-amine(BOA) and ortho-hydroxybenzaldehyde.The structure of Boz-BOA was confirmed by FTIR and ~1H NMR spectra.The DSC was utilized to probe the curing behavior of Boz-BOA and exhibited a narrow melting peak and curing exothermic peak.
作者 Po Yang,Yi Gu State Key Laboratory of Polymer Materials Engineering,College of Polymer Science and Engineering, Sichuan University,Chengdu 610065,China
出处 《Chinese Chemical Letters》 SCIE CAS CSCD 2010年第5期558-562,共5页 中国化学快报（英文版）
基金 supported by the National Natural Science Foundation of China(No.20774060)
关键词 BENZOXAZINE BENZOXAZOLE SYNTHESIS CHARACTERIZATION Benzoxazine Benzoxazole Synthesis Characterization
分类号 O626.2 [理学—有机化学]
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参考文献10

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  • 2赵培,朱蓉琪,顾宜.苯并噁嗪/PEI共混体系性能的初步研究[J].材料工程,2009,37(S2). 被引量：5
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  • 5Agag T, Takeiehi T, Synthesis and Characterization of Novel Benzoxazine Monomers Containing Allyl Groups and Their High Performance Thermosets[J]. Macromole- cules, 2003, 36 (16) : 6010-6017.
  • 6Chemykh A, Liu J P, Ishida H. Synthesis and Properties of a New Crosslinkable Polymer Containing Benzoxazine Moiety in the Main Chain[J]. Polymer, 2006, 47 (22) : 7664 -7669.
  • 7Zumiga C, Lligadas G, Ronda J C, et al. Sell'foaming Di- phenolic Acid Benzoxazine[J]. Polymer, 2012, 53 ( 15 ): 3089-3095.
  • 8Kiskan B, Colak D, Muftuoglu A, et al. Synthesis and Characterization of Thermally Curable Benzoxazine Func- tionalized Polystyrene Macromonomers[J]. Macromol Rapid Communication, 2005,26(10) : 819-824.
  • 9Herrera Velez P, Doyama K, Abe H, et al. Synthesis and Characterization of Highly Fluorinated Folymer with the Benzoxazine Moiety in the Main Chain[J]. Macromole cules, 2008,41 (24): 9704-9714.
  • 10Yagci Y, Kiskan B, Ghosh N N. Recent Advancement on Polyhenzoxazine a Newly Developed High Performance Thermoset[J]. Polymer Science Part A: Polymer Chemis- try, 2009,47(21) : 5565-5576.

引证文献4

二级引证文献11

Chinese Chemical Letters
2010年 第5期

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