摘要
The title compound was crystallized in the monoclinic system, spacegroup P21/c(#14), with a= 9. 201 (1), b= 17. 690 (4), c= 10. 949 (4) A, β=108. 97(1)°, V= 1685. 4 A3, D. = 1. 46 g/cm3, Z= 2, Mr = 755. 76, λ(MoKa) =0. 71073A, μ= 13. 2 cm-1, F(000) = 748, final R= 0. 055 and R.= 0. 058 for 1056observable reflections with I≥3δ(I). In the complex each Cu atom is coordinated byfour bridging bidentate benzoate ligands and one THF.
The title compound was crystallized in the monoclinic system, spacegroup P21/c(#14), with a= 9. 201 (1), b= 17. 690 (4), c= 10. 949 (4) A, β=108. 97(1)°, V= 1685. 4 A3, D. = 1. 46 g/cm3, Z= 2, Mr = 755. 76, λ(MoKa) =0. 71073A, μ= 13. 2 cm-1, F(000) = 748, final R= 0. 055 and R.= 0. 058 for 1056observable reflections with I≥3δ(I). In the complex each Cu atom is coordinated byfour bridging bidentate benzoate ligands and one THF.
