摘要
he single crystal of a tetra-component heteropoly compound Mo_2Co_3O_(68) (H_2O_2)_2 ] [MoO_6]. 15(H_2O) was obtained in an aqueous solution with Na_2MoO_4 , Na_2WO_4, Co (NO_3)_2 and H_3PO_4 as starting materials. The erystallo-graphic data determined by means of X-ray diffraction analysis are: triclinic sys -tem,space group Pl ,Z= 2:a =1.9227(9) nm,b=1.9359(7)nm , c=1.2565(3)nm . a = 91. 43 (3), The Differential thermal and thermogravimetric analysis indicated the thermal stbility of the compound and its spectral properties were characterized by IR and XPS measurements .
he single crystal of a tetra-component heteropoly compound Mo_2Co_3O_(68) (H_2O_2)_2 ] [MoO_6]. 15(H_2O) was obtained in an aqueous solution with Na_2MoO_4 , Na_2WO_4, Co (NO_3)_2 and H_3PO_4 as starting materials. The erystallo-graphic data determined by means of X-ray diffraction analysis are: triclinic sys -tem,space group Pl ,Z= 2:a =1.9227(9) nm,b=1.9359(7)nm , c=1.2565(3)nm . a = 91. 43 (3), The Differential thermal and thermogravimetric analysis indicated the thermal stbility of the compound and its spectral properties were characterized by IR and XPS measurements .
