正已基膦酸单正已酯及其衍生物的合成

Synthesis of n-HexyL n-HexyLphosphonates and Their Derivatives

本文参照文献方法,在先制备烷基亚膦酸单酯后,利用Todd反应合成了一系列新的正己基膦酸单正己酯及其衍生物。经过元素分析、层析、折光、红外光谱和核磁共振等测定方法鉴定了合成产品,这些化合物可望在化工和湿法冶金中获得良好的应用前景。

<ABSTRACT>: Following the methods published in literature,a series of new n-hexyl n-hexylphosphonates and tneir derivatives are synthesized by the Todd reaction on the basis of the preperation of alkyl alkylphosphonate. Tne products are identified by element analysis, chromatography, refraction, infrared spectrum ,and nuclear magnetic resonance,etc. These compounds may be used respectively in chemical and hydrometallurgical industries.