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Electronic microscopy analysis of HAP single crystals prepared by hydrothermal method 被引量:1

Electronic microscopy analysis of HAP single crystals prepared by hydrothermal method
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摘要 Hydroxyapatite(HAP, Ca 10(PO 4) 6(OH) 2) is one of the quite important bone implant materials. The hydroxyapatite crystals were synthesized under hydrothermal condition. The specimen was verified to be HAP crystal by the X-ray powder diffractometry(XRD). Then the specimen was distinguished single crystal from polycrystal by the use of the transmission electron microscope(TEM). The diffraction pattern of the specimen is neatly arranged diffraction spots, that verified the crystals were single crystals. The interplanar distance d calculated from diffraction spot is coincided with that of HAP’s JCPDS card. Moreover, crystal face angles calculated from crystal face index are coincided with the values by measuring on the pattern. The HAP crystals are needle-like in shape with about 3 μm in diameter and 180 μm in length. Most of the crystals are separate whiskers. Their length/diameter ratio ranges from 40 to 100. The average ratio is about 60. Hydroxyapatite(HAP, Ca 10(PO 4) 6(OH) 2) is one of the quite important bone implant materials. The hydroxyapatite crystals were synthesized under hydrothermal condition. The specimen was verified to be HAP crystal by the X-ray powder diffractometry(XRD). Then the specimen was distinguished single crystal from polycrystal by the use of the transmission electron microscope(TEM). The diffraction pattern of the specimen is neatly arranged diffraction spots, that verified the crystals were single crystals. The interplanar distance d calculated from diffraction spot is coincided with that of HAP's JCPDS card. Moreover, crystal face angles calculated from crystal face index are coincided with the values by measuring on the pattern. The HAP crystals are needle-like in shape with about 3 μm in diameter and 180 μm in length. Most of the crystals are separate whiskers. Their length/diameter ratio ranges from 40 to 100. The average ratio is about 60.
出处 《中国有色金属学会会刊:英文版》 CSCD 2003年第1期69-72,共4页 Transactions of Nonferrous Metals Society of China
基金 Project( 99J0 76 )supportedbytheNaturalScienceFoundationofHubei,China
关键词 HAP 羟基磷灰石 单晶水热法 衍射图 电子显微镜 hydroxyapatite single crystal hydrothermal method diffraction pattern
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