摘要
以季戊四醇和三氯氧磷为原料,在超声条件下合成季戊四醇双磷酰氯,显著降低反应温度,加快了反应速度,提高反应收率。分析结果确证反应产物为目标产物。
Pentaerythritol phosphonyl dichloride was prepared from phosphoryl chloride and pentaerythritol by ultrasonic irradiation. Result showed that both temperature and time of reaction were reduced and the structure of product was supported by analytical date.
出处
《云南化工》
CAS
2004年第3期4-6,共3页
Yunnan Chemical Technology