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对联苯二酚桥联环糊精键合硅胶固定相的合成与色谱性能测试 被引量：2

Preparation and Characterization of 4,4-Dihydroxydiphenyl-Joined β-Cyclodextrin Bonded Silica Stationary Phase for High Performance Liquid Chromatography
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摘要 合成对联苯二酚桥联环糊精键合硅胶固定相;利用傅里叶红外光谱、X射线光电子能谱、莫氏(Molisch)颜色实验进行了表征;以邻苯二甲酸二甲酯、甲苯和菲为测试溶质,评价该键合固定相的色谱性能,并考察了该固定相对一些位置异构体的色谱分离效果;讨论了可能的分离机理. A 4,4-dihydroxydiphenyl-bridged β-cyclodextrin bonded stationary phase(β-CD-D2-CSP) was prepared. The resulting bonded silica has been characterized by various methods. The chromatographic performances of β-CD-D2-CSP used for isomers' separation were investigated, and their mechanism of retention was discussed.
作者 罗爱芹 刘立文 戴荣继 张金专 方敏
机构地区 北京理工大学生命科学与技术学院
出处 《北京理工大学学报》 EI CAS CSCD 北大核心 2004年第7期646-649,共4页 Transactions of Beijing Institute of Technology
关键词 高效液相色谱 对联苯二酚桥联环糊精 键合硅胶 固定相 high performance liquid chromatography 4,4-dihydroxydiphenyl-bridged β-Cyclodextrin bonded silica stationary phase
分类号 O657.72 [理学—分析化学]
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参考文献3

  • 1[1]Armstrong D W, Jin H L. Evaluation of the liquid chromatographic separation of monosaccharides, disaccharides, trisaccharides, tetrasaccharides, de oxysaccharides and sugar alcohols with stable cyclodextrin bonded phase columns[J]. J Chromatogr, 1989,462:219-232.
  • 2[2]Hargitai T, Kaiday, Okamoto Y. Preparation and chromatographic evaluation of 3,5-di methylphenyl carbamoylated β-cyclodextrin stationary phases for normal-phase high-performance liquid chromato-graphy separation of enantionmers[J]. J Chromatogr, 1993,628(1):11-22.
  • 3[3]Bonomo R P, Cucjnotta V, Alessandro F D. Conformational feature and coordination properties of functionalized cyclodextrins[J]. Inorg Chem,1991,30:2708-2713.

同被引文献26

  • 1万军民,胡智文,陈文兴,陈海相,余志成.纤维素纤维接枝β-环糊精的合成及其富集金属离子研究[J].高分子学报,2004,14(4):566-572. 被引量：31
  • 2艾萍,韩丽娜,字敏,孟磊,字富庭,袁黎明.桥联β-环糊精液相色谱键合固定相研究[J].分析化学,2006,34(10):1459-1462. 被引量：14
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  • 4Matsui,Y., Kurita,T., Yagi,M.Bull.Chem.Soc.Jpn.,1975,48(7):2187.
  • 5Armstrong,D.W., Li,W.Y., Chang,C.D.Anal.Chem.,1990,62:914.
  • 6Hargitai,T., Okamoto,Y.J.Liq.Chromatogr.,1993,16(4):843.
  • 7Chankvetadze,B., Yashima,E., Okamoto,Y.J.ChromatogrA,1994,670:9.
  • 8Yin Xiao,Siu-Choon Ng,Timothy Thatt Yang Tan,Yong Wang.Recent development of cyclodextrin chiral stationary phases and their applications in chromatography[J].Journal of Chromatography A.2012
  • 9Xia Li,Zhi-Ming Zhou,Di Xu,Jun Zhang.Enantiomeric separation in high-performance liquid chromatography using novel β-cyclodextrin derivatives modified by R-configuration groups as chiral stationary phases[J].Talanta.2011(4)
  • 10Xianghua Lai,Weihua Tang,Siu-Choon Ng.Novel cyclodextrin chiral stationary phases for high performance liquid chromatography enantioseparation: Effect of cyclodextrin type[J].Journal of Chromatography A.2011(33)

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北京理工大学学报
2004年 第7期

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