期刊文献+

超声波辐射下β-吲哚衍生物的合成 被引量:8

Synthesis of β-Indole Derivatives under Ultrasound Irradiation
下载PDF
导出
摘要 在超声波下以吲哚、芳香醛、丙二酸亚异丙酯为原料一锅法合成了 β 吲哚衍生物——— 5 [( 3 吲哚基 ) 芳甲基 ] 2 ,2 二甲基 1 ,3 二氧六环 4,6 二酮 ,其结构经IR和1HNMR确认。 Indole derivatives——5-[(indole-3-yl)-arylmethyl]-2,2-dimethyl-1,3-dioxane-4,6-dione were synthesized from indole, aromatic aldehyde and isopropylidene malonates under ultrasound irradiation in one-step. Their structures were confirmed by IR and 1H NMR.
出处 《合成化学》 CAS CSCD 2004年第5期505-507,共3页 Chinese Journal of Synthetic Chemistry
关键词 吲哚 芳香醛 丙二酸亚异丙酯 超声波 indole aromatic aldehyde isopropylidene amalonates ultrasounic wave
  • 相关文献

参考文献4

  • 1Selic L,Stanovnik B. Dimethylamine Substitution in N,N-Dimethyl Enamines. Synthesis of Aplysinopin Analogues and 3-Aminotetrahydrocoumarin Derivatives[J].Tetrahedron,2001,57:3159-3164.
  • 2Yuji Oikawa,Hitoshi Hirasawa,Osamu Yonemitsu. Meldrum's Acid in Organic Synthesis: A One-pot Synthesis of Ethyl Indolepropionates[J].Tetrahedron Letters,1978,20:1759-1762.
  • 3Csaba Nemes,Laurent Jeannin,Janos Sapi. A Conveninent Synthesis of Conformationally Constrained β-substituted Tryptophans[J].Tetrahedron,2000,56:5479-5492.
  • 4Davidson D,Bernhardt S A. The Structure of Meldrum's Supposed β-Lactonic Acid[J].J Am Chem Soc,1948,70:3426-3428.

同被引文献66

  • 1Farhad SHIRINI,Nader Ghaffari KHALIGH.无溶剂条件下N-磺酸琥珀酰亚胺催化乙酰化反应(英文)[J].催化学报,2013,34(4):695-703. 被引量:6
  • 2Du, DM,Meng, SM,Wang, YM,Meng, JB,Zhou, XZ.Solid state reaction of aromatic ketones with heteroaromatics[J].Chinese Journal of Chemistry,1995,13(6):520-524. 被引量:1
  • 3屈彬,赵德丰.利用煤焦油中的吲哚制取芦竹碱[J].燃料与化工,2005,36(2):46-47. 被引量:2
  • 4李记太,代红光,蔺志平.3-取代吲哚衍生物的合成[J].化学进展,2007,19(5):751-761. 被引量:23
  • 5Dmling A,Wang W,Wang K.Chemistry and biology of multicomponent reactions[J].Chem Rev,2012,112(6):3083-3135.
  • 6Epifano F,Genovese S,Rosati O,et al,Ytterbium triflate catalyzed synthesis ofβ-functionalized indole derivatives[J].Tetrahedron Lett,2011,52(5):568-571.
  • 7Nemes C,Jeannin L,Sapi J,et al.A convenient synthesis of conformationally constrainedβ-substituted tryptophans[J].Tetrahedron Lett,2000,56(30):5479-5492.
  • 8Stéphane G,Bérangère L,Antonella F,et al.Multicomponent reactions studies:Yonemitsu-type trimolecular condensations promoted by Ti(Ⅳ)derivatives[J].Tetrahedron,2010,66(16):3065-3069.
  • 9Armstrong E L,Grover H K,Kerr M A.Scandium trilate-catalyzed nucleophilic additions to indolylmethyl meldrum's acid derivatives via a Gramine-type fragmentation:synthesis of substituted indolemethanes[J].J Org Chem,2013,78(20):10534-10540.
  • 10Oikawa Y,Hirasawa H,Yonemitsu O.Meldrum's acid in organic synthesis:A convenient one-pot synthesis of ethyl indolepropionates[J].Tetrahedron Lett,1978,19(20):1759-1762.

引证文献8

二级引证文献37

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部