摘要
用水热法合成 3-吡啶四唑 ,考察了不同反应条件对产率的影响 ,优化出最佳反应条件 ,产率可达 74 .1%。
pyridyltetrazole was prepared in the presence of ZnCl 2 and NaN 3 in water. The optimum condition was obtained and the yield could reach 74.1 %.
出处
《山西化工》
2004年第3期22-23,共2页
Shanxi Chemical Industry
关键词
水热法
合成
3-吡啶四唑
hydrothermal method
synthesis
3-pyridyltetrazole