耐热炸药1，3-二（3’-氨基，2’，4’，6’-三硝基苯胺基）-2，4，6-三硝基苯的合成研究

Synthesis of heat - resistant Explosive 1,3-bi (3′-amino, 2′, 4′, 6′ - trinitroanilino) -2,4,6-trinitrobenzen

成功的合成了1,3-二(3′氨基,2′,4′,6′-三硝基苯胺基)-2,4,6-三硝基幕,通过质谱、元素分析及核磁共振证明了中间体和产品的结构,并研究了反应时间、温度、催化剂及反应体系pH值对反应过程的影响.

1,3-bi(3′-amino,2′,4′,6′-trinitroanilino) -2,4,6-trinitrobenzen has been synthesized in this paper. The result of product by elementary analysis is identical with that of 1,3-bi(3′-amino,2′,4′,6′-trinitroanilino) -2,4,6-trinitrobenzen. MS and NMR spectrum show product is 1,3-bi(3′-amino,2′,4′,6′trinitroanilino) -2,4,6-trinitrobenzen. The influence of time, temperture and catalysis on step reactions is studied.