摘要
2,2,3,3-tetrafluoropropyl acrylate(TFPA)was prepared by esterification of acrylic acid and 2,2,3,3-tetrafluoropropanol in the presence of polymerization retarder,dehydration agent and concentrated sulfuric acid.The effect of polymerization retarader,the amount of sulfuric acid and reaction duration on the yield of TFPA was reported.The results showed that the yield of TPFE was 65～70% based on the theoretical calculation under optimized experimental conditions.
2,2,3,3-tetrafluoropropyl acrylate(TFPA)was prepared by esterification of acrylic acid and 2,2,3,3-tetrafluoropropanol in the presence of polymerization retarder,dehydration agent and concentrated sulfuric acid.The effect of polymerization retarader,the amount of sulfuric acid and reaction duration on the yield of TFPA was reported.The results showed that the yield of TPFE was 65～70% based on the theoretical calculation under optimized experimental conditions.
出处
《化学研究与应用》
CAS
CSCD
北大核心
2004年第5期671-672,共2页
Chemical Research and Application
关键词
2
2
3
3-四氟丙醇
含氟丙烯酸酯
氟化丙烯酸酯
合成
2,2,3,3-tetrafluoropropyl acrylate
fluorine-containing acrylate
fluorinated acrylate
preparation.
