摘要
采用固定相为301釉化担体/阿皮松L/聚乙二醇-20M-2-硝基对苯二甲酸(100/10/0.65,质量比)的气相色谱仪,并配以质谱法、IR法和NMR法,对由1,3-二氯-2-丁烯氯化制取的2,3,4-三氯-1-丁烯轻脱氯化氢的馏分进行了全分析,确定出15个组分及其含量。
The distillate of dehydnxhlorination of 2,3,4-trichloro-1 - butene , chlorinated from 1,3-dichloro-2-butene was completely determined by gas chromatography coordinated with mass spectrornetry, infrared spectroscopy and nuclear magnetic resonance spectroscopy. Fifteen components in the distillate were separated completely by a column packed with 301 glazed supporter/Apiezon L/carbowax-20 M-2-nitro-terephthalic (100/10/0.65 mass) and the composition of distillate was determined by the area normalization method.
出处
《合成橡胶工业》
CAS
CSCD
北大核心
1993年第4期232-233,共2页
China Synthetic Rubber Industry
关键词
三氯丁烯
二氯丁二烯
氯化氢
光谱
2,3,4-trichloro-l-butene
2,3- dichloro -1,3-butadiene
complete analysis
gas chromatography
mass spectrometry
infrared spectroscopy
nuclear magnetic resonance spectroscopy
