3-胺基-N-(9′-癸烯基)水杨酰胺的合成研究(Ⅱ)

THE SYNTHESIS OF 3-AMINOSALICYL-N-(9'-DECENYL) AMIDE

用改进的方法,以十一烯酸和硝基水杨酸为原料,经史米特(Schmidt)重排,还原,酯化,缩合反应制备新化合物3-胺基-N-(9′-癸烯基)水杨酰胺。产品结构经IR,~1H NMR和MS鉴定。

The new 3-Aminosalicyl-N-(9'-decenyl) amide was prepared by an improved method from 10-undecenoic acid and 3-nitrosalicylic acid through Schmidt rearrangement, reduction, esterification and condensation. The structure was established by IR, ~1H NMR and MS spectra.