Analysis of the Aconitine Alkaloids in Chuanwu by Electrospray Ionization/Tandem Mass Spectrometry
Analysis of the Aconitine Alkaloids in Chuanwu by Electrospray Ionization/Tandem Mass Spectrometry
摘要
An electrospray ionization / tandem mass spectrometric (ESI/MS/MS) method was developed for the simultaneous identification and analysis of three aconitine alkaloids [ mesacontine (MA), hypaconitine (HA), and aconitine (A)] as intact molecules at low nanogram level in Chinese traditional medicine Chuanwu decoction as well as in human whole blood extract without chromatographic separation.
参考文献7
-
1H.Y.Hsu,Y.P.Chen,S.J.Sheu.OrientalMateriaMedica, aConciseGuide[]..1986
-
2P.P.H.But,Y.T.Tai,K.Young. Vet Hum.Tox . 1994
-
3P.P.H.But,A.M.Sun,Y.S.Wong, et al. J.Chin.Med . 1994
-
4T.Y.Chen,B.Tomlinson,C.S.Cockram. Vet Hum.Tox . 1994
-
5R.Gimet,A.Filloux. Journal of Chromatography . 1979
-
6A.M.Sun,D.H.Chen,P.X.Bi. ChinJ.Chromatogr . 1999
-
7A.M.Sun,Z.M.Huang. SecondAsia-PacificInternationalSymposium onCapillaryElectrophoresis andRelatedMicroscaleTechniques . 1998
-
1李正邦,吕光华,陈东林,王锋鹏.草乌中生物碱的化学研究[J].天然产物研究与开发,1997,9(1):9-14. 被引量：46
-
2李志勇,李彦文,孙建宁,张硕峰.乌头类植物药三种双酯型生物碱研究进展[J].中央民族大学学报（自然科学版）,2009,18(2):87-91. 被引量：23
-
3陈洪超,王宪楷,赵同芳,廖循.中坝鹅掌叶附子中的生物碱成分[J].天然产物研究与开发,2003,15(4):324-325. 被引量：16
-
4孙太欣,彭国光,薛鹏,杨福全.帕金森病患者脑脊液蛋白质组学分析[J].中国生物化学与分子生物学报,2010,26(1):62-70. 被引量：1
-
5李治滢,陈有为,杨丽源,李绍兰,吴少华.川乌植物内生真菌抗菌活性的研究[J].天然产物研究与开发,2009,21(4):676-678. 被引量：10
-
6王晓东,袁小红,杨海君,侯大斌,王惠,许源.3,13-酯基中乌头碱衍生物的合成及其杀虫活性的研究[J].安徽农业科学,2009,37(21):9830-9831. 被引量：4
-
7许源,侯大斌,杨海君,袁小红,王惠,赵祥升.中乌头碱衍生物的合成及其杀虫活性测定[J].安徽农业科学,2009,37(9):3890-3892. 被引量：1
-
8Hong Kan,Wen-Yue Jiang,Ru Ding,Zhong-Ying Liu,Zi-Feng Pi,Zhi-Qiang Liu.Studies of the intestinal absorption of the alkaloids in the Wu-tou decoction combined with different incompatible medicinal herbs in a Caco-2 cell culture system using UPLC-MS/MS[J].Chinese Chemical Letters,2015,26(5):590-594. 被引量：5
-
9LIU Cheng-bai,TIAN Luo,YU Zhen-xiang,ZHANG Feng-chun,CHEN Xia.Effects of Solvents on Extraction of Effective Components from Cell Wall Tissues of Chinese Traditional Medicines[J].Chemical Research in Chinese Universities,2009,25(6):899-903.
-
10熊江,古昆,谭宁华.黑顺片的二萜生物碱成分[J].天然产物研究与开发,2008,20(3):440-443. 被引量：8
