氨—次氯酸钠法合成偏二甲肼的研究

SYNTHESIS OF N,N-DIMETHYLHYDRAZINE

研究了氨一次氯酸钠法合成偏二甲肼的反应,探索出本合成法的最佳反应条件,收率达87％。对影响因素进行了初步讨论。

N,N-dimethylhydrazine is synthesised via the reactions of ammonia, hypochloride and dimethylamine, with the yield up to 87%, higher than the known reports in published articles , and the influential factors are discussed.