The Synthesis of Bis(carboxyalkylmethyl) Diselenides by Selenium Transfer Reaction of Aryl Selenoamides
The Synthesis of Bis(carboxyalkylmethyl) Diselenides by Selenium Transfer Reaction of Aryl Selenoamides
参考文献8
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5[5]Representative data: 4b: oil6; 1H NMR (CDCl3 (ppm): 3.85 (q, 2H, J=7.2 Hz, CH2), 3.54 (s, 2H, CH2), 1.07 (t, 3H, J=6.9 Hz, CH3); IR (KBr): 3000, 2960, 1745, 1264, 1100, 1030 cm-1; MS (70 eV) m/z (%): 334 (M+, 10.51), 286 (6.34), 254 (4.41), 208 (10.06), 181 (10.72), 153 (9.51), 121 (16.74), 93 (19.51), 59 (55.34), 42 (100);Anal. calcd. for C8H14O4Se2: C 28.93, H 4.25; Found C 28.81, H 4.34.
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