摘要
在无催化剂无溶剂微波辐射下用芳香醛和 1,3 二氨基硫脲合成了双缩二氨基硫脲类化合物 ,为该类化合物提供了一种新的简便合成方法 .
The microwave-enhanced synthesis of thiocarbonohydrazones from aromatic aldehydes and thiocarbonohydrazide under solvent-free conditions without catalyst was achieved. This method is a good option to obtain the title compounds in a simple and inexpensive way. Their structures were confirmed by 1H NMR and IR spectra.
出处
《有机化学》
SCIE
CAS
CSCD
北大核心
2004年第11期1472-1474,共3页
Chinese Journal of Organic Chemistry
基金
陕西省教育厅专项基金 (No.0 1JK2 0 5)资助项目 .