摘要
A method of the determination of butylcinnamyl in human tissue was developed.The samples were extracted by L-L extraction method. The parameters of gas chromatography-mass spectrometry (GC/MS) were optimized. The method possess less-disturb,high recovery and good-reproduction. The work curve is area=842 4.77 ×content (ng/μL)-790. 714, area is linear with content between 1μg/mL to 20μg/mL. Correlation factor R is 0. 998, average recovery is 93.8% and RSD is 2.82% ; Content of butylcinnamyl in liver tissue is 0. 03μg/g, RSD is 4.17%.
出处
《质谱学报》
EI
CAS
CSCD
2004年第B10期153-154,共2页
Journal of Chinese Mass Spectrometry Society