摘要
报道了四苯乙烯基卟啉的简易合成。在醋酸锌存在下 ,在 N2 保护下通过肉桂醛和吡咯在醋酸中直接缩合 ,合成了目标化合物。用 1H NMR、UV- Vis。
In this paper, synthesis of tetrastyreneporphyrin (TStPPH-2) with a simple and easy method was reported, which was synthesized by direct condensation of aldehyde and pyrrole in acetic acid under N-2 with zinc acetic added firstly. The target molecule was characterized by +1H NMR, MS, UV-Vis spectra and elementary analysis.
出处
《化学通报》
CAS
CSCD
北大核心
2004年第11期853-854,852,共3页
Chemistry
基金
国家自然科学基金 (2 0 376 0 18
2 0 4 36 0 10 )
教育部博士点基金资助项目